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1.0 ABSTRACT 1
2.0 INTRODUCTION 2
3.0 PROJECT CHARTER 4
4.0 CONCEPT ASSESSMENT 5
4.1 MARKET AND COMPETITIVE ANALYSIS 5
4.2 CUSTOMER REQUIREMENTS 6
4.3 INNOVATION MAP 7
4.4 PRELIMINARY PROCESS SYNTHESIS 8
4.5 ASSEMBLY OF DATABASE 9
4.6 BENCH-SCALE LABORATORY WORK 9
5.0 PROCESS FLOW DIAGRAMS & MATERIAL BALANCES 10
5.1 SECTION 100 11
5.2 SECTION 200 13
5.3 SECTION 300 15
5.4 SECTION 400 17
5.5 SECTION 500 21
6.0 PROCESS DESCRIPTION 23
7.0 REACTOR DESIGN 34
6.1 REACTION ONE 34
6.2 REACTION TWO 36
6.3 REACTION VESSEL CALCULATIONS 37
6.4 REGENERATION OF CATALYST 42
8.0 ENERGY BALANCE & UTILITY REQUIREMENTS 44
9.0 UNIT DESCRIPTIONS 50
9.1 COMPRESSORS 50
9.2 DISTILLATION COLUMNS 50
9.3 DECANTERS 52
9.4 HEAT EXCHANGERS 52
9.5 PRESSURIZED VESSELS 56
9.6 FIRED HEATERS 58
9.7 PUMPS 58
9.8 PRESSURE SWING ADSORPTION UNITS 61
9.9 REACTION VESSELS 61
9.10 REFLUX ACCUMULATORS 62
9.11 MIXERS AND SPLITTERS 63
9.12 STORAGE TANKS 63
9.13 VALVES 64
10.0 COST SUMMARIES 65
10.1 EQUIPMENT COST SUMMARY 65 Table of Contents Burla, Fehnel, Louie, Terpeluk

10.2 FIXED CAPITAL SUMMARY 67
10.3 VARIABLE COST SUMMARY 69
10.4 FIXED COST SUMMARY 71
11.0 ECONOMIC ANALYSIS 73
12.0 OTHER IMPORTANT CONSIDERATIONS 79
12.1 PLANT STARTUP 79
12.2 PROCESS SAFETY 79
12.3 ENVIRONMENTAL CONCERNS 79
12.4 PROCESS CONTROLLABILITY 80
13.0 CONCLUSIONS 81
14.0 ACKNOWLEDGEMENTS 83
15.0 BIBLIOGRAPHY 84
APPENDICES 86
APPENDIX A: DISTILLATION TOWER OPTIMIZATION 86
APPENDIX B: MATLAB CODE FOR R-101 OPTIMIZATION 89
APPENDIX C: SAMPLE DESIGN AND COST CALCULATIONS 90
APPENDIX D: UNIT SPECIFICATION SHEETS 96
APPENDIX E: SAMPLE ASPEN SIMULATION RESULTS 140
APPENDIX F: MATERIAL SAFETY DATA SHEETS 160
APPENDIX G: EXCEL SHEETS FOR ECONOMIC ANALYSIS 185
APPENDIX H: PROBLEM STATEMENT


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